On Monday, November 28, 2016 the web course LC-MS Method Validation was launched for the first time as a MOOC (Massive Online Open Course). There are 301 registered participants from 61 countries, ranging from Vietnam to Peru and from Norway to Zambia. Image on the left shows the countries where the participants come from.
This is a practice-oriented on-line course on validation of analytical methods, specifically using LC-MS as technique. The course introduces the main concepts and mathematical apparatus of validation, covers the most important method performance parameters and ways of estimating them. The course follows the tradition set by the course Estimation of Measurement Uncertainty in Chemical Analysis launched in 2014. Differently from the uncertainty course, the LC-MS validation course is delivered by a team of 8 teachers, each with their own specific area of competence. This way it is expected to offer the best possible knowledge in the different subtopics of analytical method validation.
The full course material is accessible from the web page https://sisu.ut.ee/lcms_method_validation/. The course materials include videos, schemes, calculation files and numerous self-tests (among them also full-fledged calculation exercises). In order to pass the course the registered participants have to take all tests and get higher than 50% score from each of them. These tests are available to registered participants via the Moodle e-learning platform. Participants who successfully pass the course will get a certificate from the University of Tartu.
It is planned to run this course as MOOC again in autumn 2017.
(Image: Wikimedia Commons)
On 25.11.2016, in the framework of the Erasmus+ International Dimension Information Days 2016 event (Vilnius, Lithuania) Ivo Leito from UT made a presentation on the Practical experience of applying for and managing the Erasmus Mundus Joint Master Degree Programme Excellence in Analytical Chemistry (EACH). In recognition of its quality the EACH programme was selected as a “Good Practice Example” by the organizers. The presentation triggered a large number of questions and intensive discussion about funding the studies of the students who do not have the Erasmus Mundus scholarships.
We are glad to announce that the 2017 admission is officially open to the Excellence in Analytical Chemistry (EACH) Erasmus Mundus Joint Master Degree programme!
This international two-year joint master degree programme educates specialists in analytical chemistry well qualified to work in industry (food, pharmaceutical, materials, energy, etc) and chemical analysis laboratories (environment, food, health, etc) worldwide. EACH provides knowledge and practical skills in both fundamental and applied aspects of modern analytical chemistry. Practical internship placement in industry or laboratories is an important part of the training.
The programme is suitable both for students who have finished their bachelor’s studies and want to continue in master’s studies, as well as for working analytical chemistry practitioners wishing to spend couple of years to bring their knowledge and skills to a new level.
The programme features generous scholarships as detailed in the Scholarships and tuition fees page.
The programme is taught by four universities: University of Tartu (UT, coordinator), Estonia; Uppsala University (UU), Sweden; University Claude Bernard Lyon 1 (UCBL), France; and Åbo Akademi University (AAU), Finland. The language of instruction is English, but students will also learn to communicate in one of the languages of the countries involved.
The online application form, admission requirements, deadlines, list of necessary documents, instructions/explanations, as well as contact data for questions are available from the EACH Admission information page.
We are glad to announce the online course LC-MS Method Validation!
It has been set up at University of Tartu during 2015-2016 and its version 1 is now accessible from the address https://sisu.ut.ee/lcms_method_validation/
The course will be offered as a Massive Open On-line Course (MOOC) during Nov 28, 2016 – Feb 09, 2017 and it is now open for registration via the above address. The course is free of charge. This is the first edition of this MOOC and it will be offered to a limited number of participants.
This is a practice-oriented on-line course on validation of analytical methods, specifically using liquid chromatography-mass spectrometry as technique, mostly (but not limited to) using the electrospray (ESI) ion source. The course introduces the main concepts and mathematical apparatus of validation, covers the most important method performance parameters and ways of estimating them. The course is largely based on the recently published two-part tutorial review:
- Tutorial review on validation of liquid chromatography–mass spectrometry methods: Part I. A. Kruve, R. Rebane, K. Kipper, M.-L. Oldekop, H. Evard, K. Herodes, P. Ravio, I. Leito. Anal. Chim. Acta 2015, 870, 29-44
- Tutorial review on validation of liquid chromatography–mass spectrometry methods: Part II. A. Kruve, R. Rebane, K. Kipper, M.-L. Oldekop, H. Evard, K. Herodes, P. Ravio, I. Leito. Anal. Chim. Acta 2015, 870, 8-28
The course contains lectures, practical exercises and numerous tests for self-testing. In spite of being introductory, the course intends to offer sufficient knowledge and skills for carrying out validation for most of the common LC-MS analyses in routine laboratory environment. The real-life analysis situations for which there are either examples or self-tests are for example pesticide analyses in fruits and vegetables, perfluororalkyl acids in water, antibiotics in blood serum, glyphosate and AMPA in surface water, etc. It is important to stress, that for successful validation experience (both in analytical chemistry as such and also specifically in validation) is crucial and this can be acquired only through practice.
This course material is available from the above address all the time and can be used via web by anyone who wishes to improve the knowledge and skills in analytical method validation (especially when using LC-ESI-MS).
On Oct 20, 2016 Ivo Leito gave presentation titled Education Activities in Metrology in Chemistry in Vinkovci (Croatia) at the conference Laboratory Competence 2016 organized by CroLab – the Croatian Association of Laboratories.
The presentation contains information about the Applied Measurement Science and Excellence in Analytical Chemistry master’s programmes et University of Tartu, about the international consortium Measurement Science in Chemistry, about the on-line course Estimation of Measurement Uncertainty in Chemical Analysis and the new on-line course LC/MS Method Validation. Also the recently published tutorial reviews were touched upon.
The presentation led to a number of new contacts and invitation to next events. Participants were impressed by the breadth of activities as well as by the very strong team working on these things at UT. In addition, Ivo Leito was interviewed by the Croatian national television.
On Wednesday 12.10.16 the EcoBalt 2016 conference – first time organized in Tartu, Estonia – finished successfully! 42 oral talks and 43 posters were offered to the more than 150 participants from more than 25 countries. The conference featured two tutorial sessions – on measurement uncertainty and on validation of LC/MS analytical methods. The mesmerizing introductory multimedia presentation by Sven Zacek about Estonian nature and the stunning closure talk about “impossible things” by Meelika Hirmo from Let’s Do It! World were certainly among the highlights of the conference.
A number of AMS and EACH students participated in the conference.
We thank all the participants for making EcoBalt 2016 a success!
Full information about the conference, including the conference programme and EcoBalt 2016 Book of Abstracts can be found at the EcoBalt 2016 website.
EcoBalt 2016 was organized by the University of Tartu with Tallinn University of Technology and Estonian Environmental Research Centre.
EcoBalt2016 received financial support from a number of sources. We thank all supporters! Without their help the conference would not have been possible.
- For organisation of international events and conferences from Estonian Ministry of Economic Affairs and Infrastructure in cooperation with the Enterprise Estonia tourism development centre from funding provided by the European Union Regional Development Fund.
- Second day of the conference was fully supported by Environmental Investment Centre.
- The following companies supported the conference: LaboChema, Ramboll, Ordior, Quantum, SyntPot, HNK, Waters, Armgate and LanLab.
In few hours the EcoBalt 2016 conference will start, for the first time in Tartu!
The EcoBalt conference series has traditions dating back to 1993 and has been envisaged from the beginning as a Baltic event. Nevertheless, this is the first time that it takes place in Estonia (previously only in Latvia and Lithuania).
We are very glad to welcome more than 160 registered participants from more than 25 countries, making it a truly international conference! The nearby countries are represented as well as e.g. Philippines, Mexico, India, China, Nepal, Sri Lanka, … A number of EACH students also participate in EcoBalt 2016!
The EcoBalt 2016 programme is very diverse: topics ranging from ultramodern environmental analytical techniques to environmental management and from nanoparticles in environment to global climate change.
EcoBalt 2016 is organised jointly by UT in collaboration with TTU and Estonian Environmental Research Centre in the framework of the ECAC consortium.
The autumn seminar of our chair will take place on 3.-4. December in Taevaskoja Puhkekeskus.
On Sept 13, 2016 Ivo Leito gave a presentation Using MOOCs for teaching analytical chemistry: experience at University of Tartu at the EuCheMS 2016 Congress (Seville, Spain).
The presentation outlined the contents and organisation of the material in the on-line course Estimation of measurement uncertainty in chemical analysis, the different ways of using the on-line material (for independent learning, for self-testing, as an information source and as a basis for running as a MOOC) and the experience of running it as a MOOC (Massive Open Online Course) at University of Tartu during the three MOOC editions in 2014 to 2016. An important part of the presentation was devoted to analyzing the pros and cons of MOOCs as a way of teaching and in particular as a way of teaching analytical chemistry (or its subdisciplines). It was concluded that MOOCs do have advantages, especially if compared to short training courses for practitioners. The talk created quite some interest and discussions after the session.
Detailed discussion of this topic has been published: I. Leito, I. Helm, L. Jalukse. Anal Bioanal Chem 2015, 407, 1277–1281.
The course material is available for all interested people from https://sisu.ut.ee/measurement/
Preparation of a new MOOC course Validation of LC-MS analysis methods is currently underway by the group of analytical chemistry. The materials of the LC-MS validation course are nearing completion and are already available online.
This week was the first study week for the new Applied Measurement Science students and EACH Erasmus Mundus. Altogether 19 students started their studies. The countries of origin of the students are Vietnam, Philippines, Russia, Serbia, Kazakhstan, China, Sri Lanka, Nepal, Nigeria, Mexico, Lithuania, Tunisia, Pakistan and Greece. During the introductory meeting an overview of the programme was given (see the slides) and a large number of questions were asked and answered, accompanied by tea/coffee and cake.
We wish successful studies to all new students!