On-line LC-MS Method Validation Course 2022-2023: Registration is open!

We are glad to announce that the seventh edition of the online course LC-MS Method Validation is open for registration (here)! The course will be offered as a Massive Open On-line Course (MOOC) during Nov 22, 2022 – Feb 03, 2023.

This is a practice-oriented on-line course on validation of analytical methods, specifically using liquid chromatography-mass spectrometry (LC-MS) as technique, mostly (but not limited to) using the electrospray (ESI) ion source. The course will also be of interest to chromatography practitioners using other detector types. The course introduces the main concepts and mathematical apparatus of validation, covers the most important method performance parameters and ways of estimating them. More information about the course can be found in Course introduction page.

Participation in the course is free of charge. Receiving digital certificate (in the case of successful completion) is also free of charge. Printed certificate (to be sent by post) is available for a fee of 60 EUR. Registration is possible until the start of the course. The course material is available from the above address all the time and can be used via web by anyone who wishes to improve the knowledge and skills in analytical method validation (especially when using LC-ESI-MS).

We are also glad to announce, that the course has been added into the BIPM (Bureau International des Poids et Mesures) e-learning platform. The BIPM is the most important international metrology organization established by the Metre Convention, through which Member States act together on matters related to measurement science and measurement standards. BIPM is also the home of the International System of Units (SI) and the international reference time scale (UTC). The Institute of Chemistry of University of Tartu is a designated institute by the BIPM since 2010.

We are sure that being on this platform, will enable more people to find our course.

Measurement uncertainty online course 9th run has successfully finished!

On May 13, 2022 the on-line course (MOOC) Estimation of measurement uncertainty in chemical analysis offered by University of Tartu finished successfully.

Eventually, altogether 851 people registered from 103 countries. 405 participants actually started the course (i.e. tried at least one graded test at least once). The overall completion rate was 28%. This, as well as the participating rate was the lowest (48%) we have seen. However, the completion rate of the participants who started the studies was 59% with 239 successfully finished participants. Although lower than we have previously see, this result can still be considered very good for a MOOC, especially for one that has quite difficult calculation exercises, which need to be done correctly with limited number of attempts for completing the course. All statistics during the 9 years can be found in the table below.

The participants were very active and asked lots of questions. The questions were often very much to the point and addressed things that are really important to analysts in their everyday work. The course has several forums (general and by topic) and during the course period the overall number of forum posts was over 500 (!) (overall number of posts, both from participants and from teachers) and the forums are still active and posts are still coming in.

We want to thank all participants for helping to make this course a success!

We plan to repeat this course again in Spring 2023.

Measurement Uncertainty online course: 843 participants from 103 countries!

On Tuesday, March 22, 2022 the web course Estimation of Measurement Uncertainty in Chemical Analysis was launched for the ninth time as a MOOC (Massive Online Open Course)!

Currently, 843 participants from 103 countries are registered – the largest number of countries the course has ever had! In the map presented on the left, the yellow color marks the countries from where participants come. True, the map is coarse and some countries are small. Therefore, not all countries are visible. We are very happy, that we have one participant also from Ukraine this year. Slava Ukraini!

The full course material is accessible from the web page https://sisu.ut.ee/measurement/uncertainty. The course materials include videos, schemes, calculation files and numerous self-tests (among them also full-fledged measurement uncertainty calculation exercises). In order to pass the course, the registered participants have to pass six graded tests and get higher than 50% score from each of them. These tests are available to registered participants via the Moodle e-learning platform.

This course is run under the umbrella of the Estonian Center of Analytical chemistry (https://www.akki.ee/) and forms a part of the measurements and chemical analysis related master programmes at UT: Applied Measurement Science (https://ams.ut.ee/) and Excellence in Analytical Chemistry (https://www.analyticalchemistry.eu/).

 

LC-MS Validation online course 6th run has finished!

On February 11, 2022 the on-line course (MOOC) LC-MS Method Validation offered by the University of Tartu finished successfully.

Eventually, altogether 850 people registered from 97 countries. Less than half, 380 participants actually started the course (i.e. tried at least one graded test at least once) and out of them 209 successfully completed the course. The overall completion rate was 25%. The completion rate of participants who started the studies was 55%. These completion rates are lower than we usually have. So, here is some food for thought for us on how we could improve the success rate…

At the same time, those participants who actually took part in the course, were very active and asked lots of questions. The questions were often very much to the point and addressed things that are really important to analysts in their everyday work. The course has several forums (general and by topic) and during the course period the overall number of forum posts was above 200 (!) (overall number of posts, both from participants and from teachers) and the forums are still active and posts are still coming in.

This active participation made teaching of this MOOC a great experience also for us, the teachers. The discussion threads gave a lot of added value to the course and some of them triggered making important modifications to the course materials, even during the course.

We want to thank all participants for helping to make this course a success!

We plan to repeat this course again in Autumn 2022.

Measurement Uncertainty online course, March 22 – May 3, 2022: Registration is open!

The 2022 edition of the web course (MOOC) Estimation of Measurement Uncertainty in Chemical Analysis will be running from March 22 to May 3, 2022. Registration is now open!

The full course material (as well as the registration link) is accessible from the web page. The course materials include videos, schemes, calculation files, and numerous self-tests (among them also full-fledged measurement uncertainty calculation exercises) and examples. Almost all areas of analytical chemistry are addressed, ranging from simple volumetric operations and titrations to sophisticated instrumental analysis, such as determining pesticide residues by LC-MS. Efforts are made in the course to address also such uncertainty sources encountered in chemical analysis that are difficult to quantify, e.g. uncertainty due to possible interference effects (incomplete selectivity).

In order to pass the course, the registered participants have to take six graded tests and get a higher than 50% score in every graded test. These tests are available to registered participants via the Moodle e-learning platform.

Participants who successfully pass the course will get a certificate from the University of Tartu. A digital certificate of completion is free of charge. A certificate of completion on paper can be requested for a fee of 60 euros.

You are welcome to distribute this message to potentially interested people!

LC-MS Method Validation web course: 854 participants from 97 countries!

On Tuesday, November 23, 2021 the web course LC-MS Method Validation was launched for the sixth time as a MOOC (Massive Online Open Course).

There are 854 registered participants (the largest number ever in this course) from 97 countries. Both numbers are the largest we have had! The countries range from Philippines to Paraguay and from Sweden to Sri Lanka. Image on the left shows the countries where the participants come from.

This is a practice-oriented on-line course on validation of analytical methods, specifically using LC-MS as technique. The course introduces the main concepts and mathematical apparatus of validation, covers the most important method performance parameters and ways of estimating them. The LC-MS validation course is delivered by a team of 8 teachers, each with their own specific area of competence. This way it is expected to offer the best possible knowledge in all the different subtopics of analytical method validation.

The full set of course materials is accessible from the web page https://sisu.ut.ee/lcms_method_validation/. The course materials include videos, schemes, calculation files and numerous self-tests (among them also full-fledged calculation exercises). In order to pass the course the registered participants have to take all tests and get higher than 50% score from each of them. These tests are available to registered participants via the Moodle e-learning platform. Participants who successfully pass the course will get a certificate from the University of Tartu.

Measurement Uncertainty online course: 925 participants from 97 countries!

On Tuesday, March 23, 2021, the web course Estimation of Measurement Uncertainty in Chemical Analysis was launched for the eighth time as a MOOC (Massive Online Open Course)!

Currently, 925 participants from 97 countries are registered – the largest audience the course has ever had! In the map present above, the orange color marks the countries with stable participation: these countries were presented in our course last year, and so are today. The yellow color denotes the countries where we, unfortunately, do not have participants this year. The green color corresponds to the countries where we did not have participants last year, but are present now. True, the map is coarse and some countries are small. Therefore, not all countries are visible. However, altogether 15 countries are added this year!

The full course material is accessible from the web page https://sisu.ut.ee/measurement/uncertainty. The course materials include videos, schemes, calculation files and numerous self-tests (among them also full-fledged measurement uncertainty calculation exercises). In order to pass the course, the registered participants have to pass six graded tests and get a higher than 50% score from each of them. These tests are available to registered participants via the Moodle e-learning platform.

This course is run under the umbrella of the Estonian Center of Analytical chemistry and forms a part of the measurements and chemical analysis related master programmes at UT: Applied Measurement Science and Excellence in Analytical Chemistry.

 

Registration is now open: Measurement Uncertainty online course starts exactly in one month!

The 2021 edition of the web course (MOOC) Estimation of Measurement Uncertainty in Chemical Analysis will be running from March 23 to May 4, 2021. Registration is now open!

The full course material (as well as the registration link) is accessible from the web page. The course materials include videos, schemes, calculation files, and numerous self-tests (among them also full-fledged measurement uncertainty calculation exercises) and examples. Almost all areas of analytical chemistry are addressed, ranging from simple titrations to sophisticated instrumental analysis, such as determining pesticide residues by LC-MS.

In order to pass the course, the registered participants have to take six graded tests and get a higher than 50% score in every graded test. These tests are available to registered participants via the Moodle e-learning platform.

Participants who successfully pass the course will get a certificate from the University of Tartu. A digital certificate of completion is free of charge. A certificate of completion on paper can be requested for a fee of 60 euros.

You are welcome to distribute this message to potentially interested people!

LC-MS Method Validation online course finished with 28% completion rate!

Altogether 791 people were registered from 86 countries. 338 participants actually started the course (i.e. tried at least one graded test at least once) and out of them 221 successfully completed the course. The overall completion rate was 28%. The completion rate of participants who actually started the studies was 65%. All statistics during the five years can be found in the table below.

Year No of registrations No of countries Active participants Completion rate: Overall Completion rate: Participants who started studies
2017 303 61 224 55% 75%
2018 424 71 236 37% 67%
2019 426 70 227 29% 55%
2020 515 77 267 31% 60%
2021 791 86 338 28% 65%

Both the overall completion rate, as well as the completion rate of those participants who actually started the course have stabilized. The latter completion rate can be considered very good by any measure. As has been the usual case with our online courses, the questions from the participants were often very interesting, often addressed things that are really important to analysts in their everyday work. Such discussions made teaching this course a great experience also for us, the teachers!

We want to thank all participants for helping to make this course a success!

We plan to repeat this course again in Autumn-Winter 2021-2022.

Our on-line LC-MS Method Validation Course 2020-2021: Registration is open!

Validation_of_LC-MS_Methods_Online_CourseWe are glad to announce that the fifth edition of the online course LC-MS Method Validation created and organised by our Analytical Chemistry group is open for registration at the address https://sisu.ut.ee/lcms_method_validation/ !

The course will be offered as a Massive Open On-line Course (MOOC) during Nov 24, 2020 to Feb 05, 2021.

This is a practice-oriented on-line course on validation of analytical methods, specifically using liquid chromatography-mass spectrometry (LC-MS) as technique, mostly (but not limited to) using the electrospray (ESI) ion source. The course will also be of interest to chromatographists using other detector types. The course introduces the main concepts and mathematical apparatus of validation, covers the most important method performance parameters and ways of estimating them. The course is largely based on the two-part tutorial review:

The course materials assembled by the members of our group include video lectures, texts, tables, schemes, practical exercises, and numerous tests for self-testing. In spite of being introductory, the course intends to offer sufficient knowledge and mathematical skills for carrying out validation for most of the common LC-MS analyses in routine laboratory environment. The real-life analysis situations for which there are either examples or self-tests are for example determination of pesticides in fruits and vegetables, perfluoroalkyl acids in water, antibiotics in blood serum, glyphosate, and AMPA in surface water, etc. It is important to stress, that for successfully carrying out validation, practical experience – both in analytical chemistry as such and also specifically in validation – is crucial and this can be acquired only through hands-on laboratory work, not via an on-line course.

Participation in the course is free of charge. Receiving a digital certificate (in the case of successful completion) is also free of charge. Printed certificate (to be sent by post) is available for a fee of 60 EUR. Registration is possible until the start of the course. The course material is available from the above address all the time and can be used via the web by anyone who wishes to improve the knowledge and skills in analytical method validation (especially when using LC-ESI-MS).